Raman spectroscopy of carbon nano-particles synthesized by laser ablation of graphite in water

 

Authors
C?rdenas Mu?oz, Juan Fernando; Cadenbach, Spyros Thomas; Paz Rojas, Jos? Luis
Format
Article
Status
publishedVersion
Description

Carbon nanoparticles (CNPs) have been synthesized by laser ablation of polycrystalline graphite in water using a pulsed Nd:YAG laser (1064 nm) with a width of 8 ns. Structural and mesoscopic characterization of the CNPs in the supernatant by Raman spectroscopy provide evidence for the presence of mainly two ranges of particle sizes: 1-5 nm and 10-50 nm corresponding to amorphous carbon and graphite NPs, respectively. These results are corroborated by complementary characterization using atomic force microscopy (AFM) and transmission electron microscopy (TEM). In addition, large (10-100 ?m) graphite particles removed from the surface are essentially unmodified (in structure and topology) by the laser as confirmed by Raman analysis.

Publication Year
2017
Language
eng
Topic
RAMAN SPECTROSCOPY
HIGH RESOLUTION ELECTRON MICROSCOPY
CARBON NANOPARTICLE
LASER ABLATION
ATOMIC FORCE MICROSCOPY
Repository
Repositorio SENESCYT
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http://repositorio.educacionsuperior.gob.ec/handle/28000/4881
Rights
openAccess
License
openAccess